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C 27 H 54 N 6 O 28 V 10 , triclinic,P   1  ‾$P&amp;#x203e;{1}$(no. 2),  a  = 11.3803(3) Å,  b  = 14.0832(4) Å,  c  = 16.2352(7) Å,  α  = 91.784(3) Å,  β  = 104.264(3) Å,  γ  = 107.112(2) Å,  V  = 2395.04(14) Å 3 ,  Z  = 2,  R   gt   ( F ) = 0.0291,  wR   ref   ( F  2 ) = 0.0810, T = 293(2) K.

The crystal structure of tris(2,3,4,6,7,8,9,10-octahydro-1 H -pyrimido[1,2- a ]azepin-5-ium) trihydrodecavanadate(V), C 27 H 54 N 6 O 28 V 10