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C 30 H 24 O 6  ⋅ CH 2 Cl 2 , orthorhombic,  Pbcn  (no. 60),  a  = 11.6965(10) Å,  b  = 13.8078(11) Å,  c  = 16.3257(14) Å,  V  = 2636.6(4) Å 3 ,  Z  = 4,  R  gt ( F ) = 0.0765,  wR  ref ( F  2 ) = 0.1487,  T  = 296(2) K.

Crystal structure of 5,17-diformyl-25,26,27,28-tetrahydroxycalix[4]arene- dichloromethane, C 31 H 26 Cl 2 O 6