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C 10 H 14 N 6 O 2 Ni 2 , monoclinic,  I 2/ m  (no. 12),  a  = 6.7377(1) Å,  b  = 7.3500(1) Å,  c  = 14.8647(2) Å,  β  = 96.051(1)°,  V  = 732.030(18) Å 3 ,  Z  = 8,  R  gt ( F ) = 0.0314,  wR  ref ( F  2 ) = 0.0996,  T  = 150.01(10) K.

The crystal structure of poly[bis( N , N -dimethylformamide-κ 1 O )-tetrakis(μ 2 -cyanido-κ 2 C : N )dinickel(II)], C 10 H 14 N 6 O 2 Ni 2