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C 42 H 65 Br 2 N 4 NiO 8.5 , monoclinic,  P 2 1 / c  (no. 14),  a  = 14.852(2) Å,  b  = 12.1965(18) Å,  c  = 14.166(2) Å,  β  = 117.755(1)°,  V  = 2270.8(6) Å 3 ,  Z  = 2,  R  gt ( F ) = 0.0449,  wR  ref ( F  2 ) = 0.1276,  T  = 296(2) K.

zeitschrift für kristallographie - new crystal structures

Crystal structure of bis[(2-(2-bromophenyl)-5-ethyl-1,3-dioxane-5-carboxylato- κ  O )-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane- κ  4  N , N′ , N′′ , N′′′ )]nickel(II) hemihydrate C 42 H 65 Br 2 N 4 NiO 8.5