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C 12 H 9 I 6 NO, monoclinic, P2 1 /n (no. 14), a = 9.2855(2) Å, b = 17.1834(4) Å, c = 12.2416(3) Å, ( = 93.258(2)°, V = 1950.1 Å 3 , Z = 4, R gt (F) = 0.0433, wR ref (F 2 ) = 0.0630, T = 120 K.

Crystal structure of 8,10-diiodo-3-(iodomethyl)-2,3-dihydro-[1,4]oxazino- [2,3,4-ij]quinolin-4-ium triiodide, [C 12 H 9 I 3 NO]·I 3 , C 12 H 9 I 6 NO