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A new metal-organic coordination polymer, [Pb(L)(adip) 0.5 ] ( 1 ) was synthesized under hydrothermal conditions by using 1-(1 H -imidazo[4,5-f][1,10]phenanthrolin-2-yl)naphthalen-2-ol (HL) and adipic acid (H 2 adip). The complex  1  was characterized by diffraction and elemental analyses. In complex  1 , the binuclear [Pb 2 L 2 ] units were formed by the OH-deprotonation bridging neighboring Pb(II) atoms, and the adipate linked the binuclear [Pb 2 L 2 ] units to form a symmetric one-dimensional chain. The 1D chain was further extended to the 2D supramolecular layer structure through π-π interactions between the L ligands.

Synthesis and structural characterization of a novel 2D supramolecular lead coordination polymer with phenanthroline derivate and adipic acid