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Reactions of aluminium isopropoxide with 2-(o-hydroxyphenyl)-benzoxazole (pbox H ) and salicylidene-4-chloroaniline (spca H ) in different molar ratios in benzene solution afforded the complexes of the types [(μ-OPr i ) 2 Al 2 (pbox) 2 (OPr i ) 2 ]  1 , [Al(OPr i )(pbox) 2 ]  2 , [Al(pbox) 3 ]  3,  [(μ-OPr i ) 2 Al 2 (spca) 2 (OPr i ) 2 ]  4 , [Al(OPr i )(spca) 2 ]  5  and [Al(spca) 3 ]  6 . All these colored solid complexes are soluble in common organic solvents and were characterized by elemental (C, H, N and Al) analysis, spectroscopic [IR ( 1 H,  13 C and  27 Al) NMR] and mass spectrometric studies. On the basis of these studies, plausible structures have been tentatively proposed for these complexes.

main group metal chemistry

Synthesis, spectroscopic [IR, ( 1 H,  13 C,  27 Al) NMR] and mass spectrometric studies of aluminium(III) complexes containing O- and N-chelating Schiff bases