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The reaction of a series of compounds, Ar 3  Ge-MR 3 ,  1 – 4  (Ar=Ph,  p -Tol,  M =Si, Ge, R=Ph, Me, tBu), with one equivalent of trifluoromethanesulfonic acid (HOTf) was investigated. The corresponding triflates were isolated in several cases. The molecular structure of Ph 3  Ge-GePh 2  OTf ( 5 ) in solid state was investigated by X-ray analysis. The triflates were converted to the corresponding chlorides under the action of ammonium chloride.

main group metal chemistry

Reaction of digermanes and related Ge-Si compounds with trifluoromethanesulfonic acid: synthesis of helpful building blocks for the preparation of Ge-Ge(Si)-catenated compounds