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Four new di- and triorganonitrato stannate complexes and related derivatives have been synthesized and characterized by infrared and Mössbauer spectroscopy. The structure of Et 4 N[NO 3 (SnClPh 3 ) 2 (SnPh 3 NO 3 )] ( 1 ) has been determined by single-crystal X-ray diffraction analysis. In the trinuclear organostannate complex, each Sn IV  atom is five-coordinated and adopts a trigonal-bipyramidal  trans -OXSnC 3  (X=O or Cl) geometry. The overall coordination environment of the Sn IV  atoms is trans-octahedral for  2  and  3  or cis-trigonal-bipyramidal for  4 . In the related derivatives, the NO 3  -  anions behave as monodentate ligands.

Et 4 N[NO 3 (SnClPh 3 ) 2 (SnPh 3 NO 3 )]: a trinuclear organostannate complex and related derivatives