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Diclofenac (DCF) is one of the most frequently detected pharmaceuticals in the aquatic environment. This study investigated the heterogeneous activation of Oxone by Co 3 O 4  nanoparticles to eliminate DCF in aqueous phase. The performance of Co 3 O 4 /Oxone process was optimized by examining the influence of various parameters such as pH levels, Co 3 O 4  dosage, oxone concentration, DCF initial concentration and the presence of inorganic anions on the degradation rate of DCF. The mechanism of the heterogeneous catalysis (Co 3 O 4 /Oxone) was also elucidated through comparing XRD patterns and Co 2p XPS spectra of Co 3 O 4  nanoparticles before and after the degradation reaction of DCF by Co 3 O 4 /Oxone process.

Degradation of Diclofenac by Co 3 O 4 -catalyzed Activation of Oxone Process