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The scope of mesoporous molecular sieves, Al-MCM-41, as catalysts in the ozone initiated fuctionalisation of higher n-alkanes at 20 ± 1 °C and ~1 atm conditions is investigated. Oxygen is introduced into carbonaceous site in the product molecule forming 2-, 3- and 4- keto- isomers as main products and carboxylic acids as minor products. The % conversion, reaction products and selectivity for the catalysed reactions are compared. In presence of catalysts, the relative selectivity towards 4-ketone is increased.

Oxidation of Higher Alkanes at Moderate Reaction Conditions with Ozone in Presence of Mesoporous Materials