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The photocatalytic degradation of 4-Chlorophenol (4-CP) in aqueous solution has been carried out with TiO 2  nanoparticles, prepared by sol-gel method. The effects of various factors, such as different calcination temperatures of TiO 2 , amount of catalysts, and intensity of light sources were attempted for the efficient degradation of 4-CP. Pt doped TiO 2  photocatalysts were also prepared by photo-reduction method and applied for 4-CP degradation. Pt-TiO 2  catalysts showed higher rate of degradation of 4-CP than the P-25, commercially available TiO 2  . Multi-wall carbon nano-tubes (CNTs) were used as solid support for TiO 2  catalysts and proved to be useful materials to speed up the settling process within 1 h after the reaction was over. The intermediate products formed during the degradation of 4-CP were identified using LC-MS.

Photocatalytic Degradation of 4-Chlorophenol Using TiO 2 and Pt-TiO2 Nanoparticles Prepared by Sol-Gel Method