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CdO + CdTiO 3  thin films were prepared on glass substrates by means of the sol-gel technique. Two Ti/Cd ratios, 0.54 and 0.67, in the precursor solutions were studied. After the dipping process, the samples were sintered in an open atmosphere during one hour at selected temperatures (T s ) in the range of 350-600 °C. The variation of T s  was in steps of 50 °C. X-ray diffraction, UV-Vis optical absorption, and atomic force spectroscopy techniques were employed for characterization. The photocatalytic activity (PA) was measured by means of the photobleaching of an aqueous solution of methylene blue (MB) after irradiation with an UV lamp. The MB concentration was determined by using optical absorption spectra, measured before and after the photobleaching process, and the Lambert-Beer principle. The best PA was obtained for films sintered at 500 °C for both Ti/Cd ratios studied, as for this T s  value the PA was very similar.

Effect of the Sintering Temperature on the Photocatalytic Activity of CdO + CdTiO 3 Thin Films