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As a highly thermally conductive PPS that is lightweight and has excellent heat dissipation is expected to be applied in various products, its peculiar filling behavior can cause molding defects such as short shots and surface cracks. To address these challenges, it is important to elucidate the filling behavior and clarify the effects of cavity shape and molding conditions. Thus, we intend to visualize the filling behavior of the high-thermal-conductivity PPS. To achieve this goal, we develop an in-process visualization system to reveal both the thermal and kinetic behaviors of the resin while it fills the cavity. In the system, a sapphire prism glass is utilized in the mold for visualization because it exhibits high strength, high heat conduction, and high infrared transmittance. A high-speed visible camera for kinetic behavior and an infrared camera for thermal behavior are utilized. With the developed system, we successfully obtained for the first time the filling behavior of high-thermal-conductivity PPS. Visualization experiments prove that the temperature of the conventional PPS gradually decreases from the tip to the rear of the flow. However, the temperature of the high-thermal-conductivity PPS drops sharply from the tip of the flow to the rear, and breakage at the flow front near the cavity wall is generated. Our interpretation is that the flow front near the cavity wall can be easily broken when it is stretched, because the ductility of the high-thermal-conductivity PPS largely decreases because of the rapid temperature drop. To suppress the formation of this breakage, we modify the cavity shape and molding conditions, and verify its suppression effect.

international polymer processing

Visualization analysis of temperature distribution in the cavity of conventional PPS and high-thermal-conductivity PPS during the filling stage of injection molding