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By means of high performance liquid chromatography (HPLC) and gel permeation chromatography (GPC), the yields of the main reaction products and the polymeric portion formed in the reaction of guaiacylglycerol-β-guaiacyl ether (GG) under various acid-catalyzed conditions were quantified as a function of reaction time. Based on their forming sequence and reaction behavior, as well as their structural characteristics, an acid-catalyzed reaction mechanism of GG with phenol was proposed.

Liquefaction Mechanism of β-O-4 Lignin Model Compound in the Presence of Phenol under Acid Catalysis. Part 2. Reaction Behaviour and Pathways