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A facile method for the synthesis of [1,2,4]triazolo[4,3- b ][1,2,4,6]thiatriazine 1-oxides  3a–h  is presented. The approach involves a reaction between  N -triazol-3-ylamidines  2a–h  and thionyl chloride in the presence of pyridine. The structures of the synthesized compounds were confirmed by spectral studies including IR,  1 H NMR,  13 C NMR, MS and elemental analysis.

Simple and efficient approach to synthesis of [1,2,4]triazolo[4,3- b ][1,2,4,6]thiatriazine- 1-oxides from N -triazol-3-ylamidines