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Several derivatives of the novel pyrimido[4′,5′:2,3][1,4]thiazepino[7,6- b ]quinoline ring system have been synthesized through cyclocondensation of 5-amino-6-methylpyrimidine-4-thiols  5a,b  and 2-chloroquinoline-3-carbaldehydes  6a–c  in the presence of K 2  CO 3  in DMF.

Synthesis of pyrimido[4′,5′:2,3][1,4]thiazepino[7,6- b ]quinolines, derivatives of a novel ring system