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A series of bis(1,2,4-triazole-3-thiols)  3a–d  were prepared by condensation reactions of arylbis(carboxymethylthio)methanes  2a–d  with thiocarbohydrazide. The starting diacids  2a–d  were prepared by reactions of aromatic aldehydes  1a–d  with thioglycolic acid. The structures of these newly synthesized compounds are characterized by elemental analysis, IR, and NMR spectroscopy.

A simple and efficient procedure for synthesis of symmetrical bis(4-amino-4 H -1,2,4-triazole-5-thiols)