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Poly( p -xylylene)s (PPX) with aliphatic substituents at the alpha position were synthesized by chemical vapor deposition (CVD) via vapor phase pyrolysis of α-chloro-1,4-xylenes, or by base-induced dehydrohalogenation of α-chloro-1,4- xylenes (Gilch route). These PPXs are soluble under ambient conditions in organic solvents. The glass transition temperature of the  tert -butyl substituted PPX is remarkably high. Good thermal stability under nitrogen was observed for the trifluoromethyl substituted PPX. A functionalized compound suitable for polymer analogous reactions is the norbornenyl substituted PPX.

Synthesis and properties of novel poly(p-xylylene)s with aliphatic substituents