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Immunoactive ionic liquids (2-hydroxyethyl)ammonium 1-R-indol-3-ylsulfanyl-acetates HN+R1R2(CH2CH2OH) ∙ -O(O)CCH2S-Ind-R3-1 (1-5), were synthesized by the reaction of (2-hydroxyethyl)amines with indol-3-ylsulfanylacetic- or 1-benzylindol-3-ylsulfanylacetic acid. 1: R 1  = R 2  = CH 2 CH 2 OH, R 3  = H; 2: R 1  = СН 3 ,R 2 =CH 2 CH 2 OH, R 3  = H; 3: R 1  = R 2  = CH 3 , R 3  = H; 4: R 1  = R 2  = CH 2 CH 2 OH, R 3  = СH 2 С 6 Н 5 ; 5: R 1  = СН 3 ; R 2  = CH 2 CH 2 OH; R 3  = СH 2 С 6 Н 5 . The structure of each compound was elucidated by IR, NMR  1 H,  13 С, and  15 N techniques and their composition was confirmed by elemental analysis. The crystal structure of tris-(2-hydroxyethyl) ammonium indol-3-ylsulfanylacetate was investigated by X-ray diffraction analysis. Immunoactive properties of the title compounds were screened.

open chemistry

Immunoactive ionic liquids based on 2-hydroxyethylamines and 1-R-indol-3-ylsulfanylacetic acids. Crystal and molecular structure of immunodepressant tris-(2-hydroxyethyl)ammonium indol-3-ylsulfanylacetate