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A method to determine the proportion of both enantiomers of 2,6-di- O -alkylgalactose in a permethylated/perethylated polysaccharide is described. It involves conversion of the monosaccharides, obtained by hydrolysis of the sample, to the corresponding diastereomeric acetylated 1-deoxy-1-(1-phenylethylamino)alditols, followed by gas chromatographic analysis. This procedure has been applied to a polysaccharide isolated from  Pterocladiella capillacea .

Absolute Configuration of 2,6-di- O -Alkylgalactose Obtained from Peralkylated Red Algal Polysaccharides