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We investigated the molecular arrangement and surface morphology of organized molecular films of the 3-arm comb polymer containing metal ion using surface pressure-area (π-A) isotherm, inductively-coupled plasma mass spectrometry (ICP-MS), in-plane and out-of plane X-ray diffraction (XRD), and atomic force microscopy (AFM). From the result of WAXD measurement of the corresponding monomer in bulk, the long hydrocarbon chains are packed hexagonally in solid-state. Compared with their monolayer on the distilled water as subphase, that of this compound on buffer solution containing Cd ion is remarkably expanded at 15 C. It is found that highly ordered layer structures and two-dimensional lattices are constructed in the organized molecular films of Cd-bridged comb polymer using in-plane and out-of plane XRD. Further, surface morphology of the LB films fabricated from the monolayers on buffer solution including Cd formed flat and smooth domains by metal-scavenging.

Solid-state Structure and Formation of Organized Films for Three-arm Amphiphilic Polymer with Metal-Scavenging Property