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Spherical C/Li4Ti5O12 anode powders were prepared by spray pyrolysis with aqueous solution. The particle characteristics of C/Li4Ti5O12 powders were determined by SEM, XRD and DTA-TG. C/Li4Ti5O12 anode powder had a spherical morphology with non aggregation and porous structure. The carbon content was around 13 wt%. XRD analysis revealed that the spinel phase was obtained by heating at 750 °C under N2 atmosphere. The discharge capacity of C/Li4Ti5O12 was 160 mAh/g at 1C. That of C/Li4Ti5O12 decreased to 90 mAh/g at 20 C. 96 % of initial discharge capacity was maintained at 1 C after 100 cycles. 85 % of it was maintained at 20 C after 300 cycles.

transactions of the materials research society of japan

Synthesis and Electrochemical Properties of C/Li&lt;sub&gt;4&lt;/sub&gt;Ti&lt;sub&gt;5&lt;/sub&gt;O&lt;sub&gt;12&lt;/sub&gt; Powders by Spray Pyrolysis