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LiFePO4 was synthesized by a microwave hydrothermal heating (MH) method. The particle size of the product prepared by the MH method is in the range from 200 to 300 μm. The LiFePO4 cathode materials thus obtained had a higher discharge capacity and better cycle performance than those of the LiFePO4 samples prepared by a conventional hydrothermal reaction.

Hydrothermal Reaction by Microwave Heating for Synthesis of LiFePO<sub>4</sub> as Cathode Material