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The organic volatile impurities (OVI’s) specifications were set in accordance with the toxicity of solvents vary from a low ppm to thousands of ppm. The static GC-HS deamination of OVI’s is now a days mature technique well established in pharmaceutical analysis [2-4]. The OVI’s are used in produced during the synthesis of drug substances and in excipients used in the GC-HS Method for Organic Volatile Impurities Determination and Quantification in Sertraline HCl API and Its Pharmaceutical Dosage Forms