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Abstrm : Tris[4-(substituted)furann-3-yl]boroxines, prepared from the corresponding 4-(substituted)-3-(tthylsilyl)furan, were converted successfully through palladiumcatalyzed cross-coupling reactions with tri-n-butylstannyl chloride to 4-(substituted)-3(m-n-butylstannyl)furans, which underwent further palladium-catalyzed reactions with organohalides to afford 3,4-disubstituted furans. Oxidation of tris[4-(substituted)furan3 yl] boroxines generated the corresponding 4subs tituted-3 (2H)furanone s .

Regiospecific synthesis of 3,4-disubstituted furans