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MoOCl4/MoO2Cl2 were reacted with 2-mercaptopyridine (IUPAC: pyridine-2-thiol)/4phenylimidazole-2-thiol (IUPAC: 4-phenyl-1,3-dihydroimidazole-2-thione)/6-mercaptopurine (IUPAC: 1,7-dihydro-purine-6-thione) in acetonitrile medium using equal/twice molar concentrations at normal temperature. The reactions yielded products: MoOCl3(C5H4NS-SNH4C5).2HCl,[1]; Mo3O3Cl12(C5H4NSSNH4C5)(CH3CN)2,[2]; Mo2OCl6(C9H7N2S)4,[3] and Mo2O2Cl8(C5H4N4S)(CH3CN),[4]. The various techniques used for characterization of compounds are: Fourier transform infrared, protron nuclear magnetic resonance, 13C nuclear magnetic resonance, liquid/gas chromatography, mass proton spectrometry and C, H, N, S, Mo, Cl analysis. The products are prone to oxidation/hydrolysis by air/ moisture, so all procedures were executed in vacuum line using dry nitrogen atmosphere. Elemental analysis and fragments recorded in mass spectrometry are in tune with the formulae proposed.

Reactions of MoOCl4 and MoO2Cl2 with Heterocyclic Thioamides