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This study aims to synthesize Ni-doped LiNixMn2-xO4 (x = 0, 0.02, 0.04, 0.06, 0.08, 0.1) by irradiation microwave-assisted reflux technique. The microstructure of the products was investigated by x-ray diffraction equipped with U-FIT program package. Results of the structural analysis show that Ni doping changed the size, crystallinity, and microstructure of LiNixMn2-xO4. The LiNixMn2-xO4 solids have a cubic structure with a space group of Fd-3 m. Increasing the content of Ni doping does not affect the structure. The average volume of LiNixMn2-xO4 is around 555 Å3 to 580 Å3. The crystallinity of the solids tends to increase with the increasing Ni content accompanied by the decrease in unit cell lattice parameters.

Structural Analysis of LiNixMn2-xO4 Prepared by Irradiation Microwave-Assisted Reflux Technique