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The oximation of a variety of aldehydes and ketones was carried out with NH2OH·HCl in the presence of oxalic acid as catalyst under reflux conditions. The reactions were performed in CH3CN with excellent yields(90-95%) of products in appropriate times (55-90 min).

Synthesis of Oximes from the Corresponding of Organic Carbonyl Compounds with NH2OH.HCl and Oxalic Acid