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An efficient, simple and regioselective monobromination of least reactive acyclic and cyclic alkanes by sodium bromide/ 98% H2SO4 is reported. The yields are high and the reactions go to completion within 15–35 min. at  40–65 oC.

NaBr/98% H2SO4: An Efficient Reagent for the Regioselective Monobromination of Least Reactive Alkanes and Cycloalkanes