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The structure and hyperfine interactions in the Bi9Ti3Fe5O27 Aurivillius compound were studied using X-ray diffraction and Mossbauer spectroscopy. Samples were prepared by the conventional solid-state sintering method at various temperatures. An X-ray diffraction analysis proved that the sintered compounds formed single phases at temperature above 993 K. Mossbauer measurements have been carried out at room and liquid nitrogen temperatures. Room-temperature Mossbauer spectrum of the Bi9Ti3Fe5O27 compound confirmed its paramagnetic properties. However, low temperature measurements revealed the additional paramagnetic phase besides the antiferromagnetic one.

Structure and Hyperfine Interactions in Aurivillius Bi9Ti3Fe5O27Conventionally Sintered Compound

Structure and Hyperfine Interactions in Aurivillius Bi₉Ti₃Fe₅O₂₇Conventionally Sintered Compound