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Partial acid hydrolysis of a new water-absorbing polysaccharide (WAP) from the family Oxalobacteraceae gave six di-, four tri-, two tetra-, two penta-, and one hexasaccharides composed of mannose, glucose, and/or galactose. The structures of oligosaccharides 1-15 were elucidated by extensive 2D NMR spectroscopic analyses. (1)H- and (13)C-NMR chemical shift assignments of oligosaccharides 1-14 are presented.

NMR Analyses of Oligosaccharides from a New Water-absorbing Polysaccharide Produced by the Family <i>Oxalobacteraceae</i>