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Heavy atom-containing molecules cause a photoreaction by a direct S 0  → T n transition. Therefore, even in a hypervalent iodine compound with a benzene ring as the main skeleton, the photoreaction proceeds under 365-400 nm wavelength light, where UV-visible spectra are not observed by usual measurement method. Some studies, however, report hypervalent iodine compounds that strongly absorb visible light. Herein, we report the synthesis of two visible light-absorbing hypervalent iodines and their photooxidation properties under visible light irradiation. We also demonstrated that the S 0  → T n transition causes the photoreaction to proceed under wavelengths in the blue and green light region.

chemical and pharmaceutical bulletin/chemical and pharmaceutical bulletin

Synthesis of Visible-Light–Activated Hypervalent Iodine and Photo-oxidation under Visible Light Irradiation &lt;i&gt;via&lt;/i&gt; a Direct S&lt;sub&gt;0&lt;/sub&gt;→T&lt;sub&gt;n&lt;/sub&gt; Transition