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A heterogeneous metal catalyst enabled the intramolecular oxidative coupling of diarylamines to form carbazoles with molecular oxygen as the sole oxidant. Rh/C had efficient catalytic activity and allowed the catalyst loading to be reduced to 0.1 mol% while maintaining excellent yields of carbazoles. This reaction is operationally simple in an open-to-air setup, and provides a green and atom-economical process for an efficient synthetic approach to N-substituted carbazoles.

chemical and pharmaceutical bulletin/chemical and pharmaceutical bulletin

Aerobic Intramolecular Oxidative Coupling Using Heterogeneous Catalyst for Synthesis of &lt;i&gt;N&lt;/i&gt;-Substituted 2,3,6,7-Tetramethoxycarbazoles