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A new method has been developed for the umpolung α-heteroarylation of ketones via an N-alkoxyenamine. The treatment of ketones with tris(heteroaryl)aluminum reagents in the presence of isoxazolidine gave the corresponding α-heteroarylated ketones in moderate to good yields.

α-Heteroarylation of Ketones <i>via</i> the Umpolung Reaction of <i>N</i>-Alkoxyenamine