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A stereoselective synthesis is described of the C5-C13 fragment (4) of myriaporone 4 (1) starting from D-glucose by a coupling of the C5-C9 aldehyde (5), prepared using a regioselective reductive ring-opening of methoxybenzylidene acetal, with the C10-C13 iodoolefin (6).

chemical and pharmaceutical bulletin/chemical and pharmaceutical bulletin

Studies on the Synthesis of Myriaporones: Stereoselective Synthesis of the C5-C13 Fragment Starting from D-Glucose via Regioselective Reductive Opening of Methoxybenzylidene Acetal.