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Four new triterpenoid saponins, ardisimamilloside C (1), 3-O-[alpha-L-rhamnopyranosyl-(1--&gt;2)-beta-D-glucopyranosyl-(1--&gt;4)-[beta -D-glucopyranosyl-(1--&gt;2)]-alpha-L-arabinopyranosyl]-3beta,16al pha,28,30-tetrahydroxy-olean-12-en, ardisimamilloside D (2), 3-O-¿alpha-L-rhamnopyranosyl-(1--&gt;2)-beta-D-glucopyranosyl-(1--&gt;4)-[beta -D-glucopyranosyl-(1--&gt;2)]-alpha-L-arabinopyranosyl]-3beta,15al pha,28,30-tetrahydroxy-olean-12-en, ardisimamilloside E (3), 3-O-[alpha-L-rhamnopyranosyl-(1--&gt;2)-beta-D-glucopyranosyl-(1--&gt;4)-[beta -D-glucopyranosyl-(1--&gt;2)]-alpha-L-arabinopyranosl]-13beta,2 8-epoxy-3beta,16alpha,29-oleananetriol, and ardisimamilloside F (4), 3-O-[alpha-L-rhamnopyranosyl-(1--&gt;2)-beta-D-glucopyranosyl-(1--&gt;4)-[beta -D-glucopyranosyl-(1--&gt;2)]-alpha-L-arabinopyranosyl]-3beta,16al pha-dihydroxy-13beta,28-epoxy-oleanan-30-oic acid were isolated from the roots of Ardisia mamillata Hance. Structure assignments were established on the basis of highresolution (HR)-FAB-MS, 1H-, 13C-, and two-dimensional (2D)-NMR spectra, and on the chemical evidence.

Ardisimamillosides C-F, Four New Triterpenoid Saponins from Ardisia mamillata.