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Novel oxidation of vitamin D 2 was achieved by an electrochemical method. Under the conditions employing a metal salt-hematoporphyrin-O 2 -cathodic reduction system, only the conjugated triene moiety of vitamin D 2 was affected, giving the cleavage products, while the double bond in the side chain remained intact.

Novel Oxidation of Vitamin D2 by an Electrochemical Method.