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Cyclic voltammetry of diazepam has been investigated in acid solution (pH 1.0) on a glassy carbon electrode. A well defined cathodic peak is observed. The interferences by the solution components on the estimation are studied. A simple, accurate, sensitive and rapid method for the determination of the drug in pharmaceutical formulations is proposed

Cyclic Voltammetric Studies of Diazepam Using Glassy Carbon Electrode-Estimation of Diazepam in Pharmaceutical Samples.