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A new methodology for chemical differentiation of one amino and four hydroxyl groups of D-galactosamine derivatives and its application for the synthesis of D-galactosamine-4-phosphate analogs of lipid A are described. Preliminary examination of biological activity revealed that the synthetic monosaccharides show mitogenic activity.

Lipid A and Related Compounds. XXVII. An Efficient Synthesis of D-Galactosamine-4-phosphate Analogs of Lipid A via a Novel Key Intermediate.