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Photoreactive derivatives of mu-conotoxin GIIIA carrying a radioactive and chromogenic diazirine have been prepared as a photoaffinity labeling reagent for muscle-type sodium channels. When the reagent was photolyzed in the presence of the eel sodium channel, radioactivity was specifically incorporated into the channel protein.

Photoaffinity Labeling of the Electroplax Sodium Channel with a Photoreactive .MU.-Conotoxin Carrying a Radioactive and Chromogenic Diazirine.