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It was confirmed that griseofulvin, sulfanilamide and theophylline form HF adducts with combining ratios of 1 : 1 (griseofulvin : HF), 1 : 2 (sulfanilamide : HF) and 1 : 3 and 1 : 2 (theophylline : HF). The thermal and other physico-chemical properties of these adducts and the recovered medicinals were investigated by differential scanning calorimetry, thermogravimetry, X-ray powder diffractometry, infrared spectroscopy and microscopy. Effective particle size reduction was achieved by desorbing HF from the adducts.

Hydrogen fluoride adduct formation of medicinal compounds and its application to particle size reduction.