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Nitrogen-15 NMR spectroscopy showed strongly upfield values of the chemical shift for one of the azo nitrogen atoms of a boronic-acid-appended azo dye: this indicated the formation of a boron?nitrogen (B?N) dative bond. The B?N dative bond was cleaved by sugar addition

Nitrogen-15 NMR Spectroscopy of Sugar Sensor with B–N Interaction as a Key Regulator of Colorimetric Signals