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The synthesis of 1-alkenylboronic acid pinacol esters via the palladium-catalyzed cross-coupling reaction of 1-alkenyl halides or triflates with bis(pinacolato)diboron [(Me4C2O2)B-B(O2C2 Me4)] was carried out in toluene at 50 °C in the presence of potassium phenoxide (1.5 equivalents) and PdCl2(PPh3)2·2PPh3 (3 mol%).

chemistry letters

Synthesis of 1-Alkenylboronic Esters <i>via</i> Palladium-Catalyzed Cross-Coupling Reaction of Bis(pinacolato)diboron with 1-Alkenyl Halides and Triflates

Synthesis of 1-Alkenylboronic Esters via Palladium-Catalyzed Cross-Coupling Reaction of Bis(pinacolato)diboron with 1-Alkenyl Halides and Triflates