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Monochlorotriazinyl β-cyclodextrin (MCT β-CD) was employed for the inclusion complexation with oils of cedarwood, clove, eucalyptus and peppermint to assess their release behavior from functionalized cotton. The process of MCT β-CD grafting was optimized using response surface methodology with three independent factors including MCT β-CD concentration, pH and curing temperature and effect of their second order interactions on dependent variables as % nitrogen content, % graft yield, tensile strength and wash durability was examined. The interaction of MCT β-CD concentration and pH had the decisive effect on the investigated dependent variables. FTIR and % retained nitrogen confirmed the substantial retention of modified host on functionalized cotton after five vigorous wash cycles. 1HNMR characterized the full entrapment of oils within MCT β-CD cavity on cotton. All the oils were substantially retained in the inclusion complexes with the MCT β-CD before and after wash than when present uncomplexed on the treated cotton. Peppermint was the slowest to fade off and cedarwood was rapid in sublimation from the cyclodextrin moieties.

Optimization of monochlorotriazine β-cyclodextrin grafting on cotton and assessment of release behavior of essential oils from functionalized fabric