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Titanium oxyhydroxy-fluoride, TiO 0.9 (OH) 0.9 F 1.2  · 0.59H 2 O rods with a hexagonal tungsten bronze (HTB) structure, was synthesized via a facile one-step solvothermal method. The structure, morphology, and component of the products were characterized by X-ray powder diffraction (XRD), thermogravimetry (TG), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution TEM (HRTEM), inductively coupled plasma optical emission spectroscopy (ICP-OES), ion chromatograph, energy-dispersive X-ray (EDX) analyses, and so on. Different rod morphologies which ranged from nanoscale to submicron scale were simply obtained by adjusting reaction conditions. With one-dimension channels for Li/Na intercalation/de-intercalation, the electrochemical performance of titanium oxyhydroxy-fluoride for both lithium-ion batteries (LIBs) and sodium-ion batteries (SIBs) was also studied. Electrochemical tests revealed that, for LIBs, titanium oxyhydroxy-fluoride exhibited a stabilized reversible capacity of 200 mAh g −1  at 25 mA g −1  up to 120 cycles in the electrode potential range of 3.0–1.2 V and 140 mAh g −1  at 250 mA g −1  up to 500 cycles, especially; for SIBs, a high capacity of 100 mAh g −1  was maintained at 25 mA g −1  after 115 cycles in the potential range of 2.9–0.5 V.

nanoscale research letters

One-Step Synthesis of Titanium Oxyhydroxy-Fluoride Rods and Research on the Electrochemical Performance for Lithium-ion Batteries and Sodium-ion Batteries