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Highly hexagonally ordered hard anodic aluminum oxide membranes, which have been modified by a thin cover layer of SiO 2  deposited by atomic layer deposition method, were used as templates for the synthesis of electrodeposited magnetic Co-Ni nanowire arrays having diameters of around 180 to 200 nm and made of tens of segments with alternating compositions of Co 54 Ni 46  and Co 85 Ni 15 . Each Co-Ni single segment has a mean length of around 290 nm for the Co 54 Ni 46  alloy, whereas the length of the Co 85 Ni 15  segments was around 430 nm. The composition and crystalline structure of each Co-Ni nanowire segment were determined by transmission electron microscopy and selected area electron diffraction techniques. The employed single-bath electrochemical nanowire growth method allows for tuning both the composition and crystalline structure of each individual Co-Ni segment. The room temperature magnetic behavior of the multisegmented Co-Ni nanowire arrays is also studied and correlated with their structural and morphological properties.

nanoscale research letters

Electroplating and magnetostructural characterization of multisegmented Co54Ni46/Co85Ni15 nanowires from single electrochemical bath in anodic alumina templates