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The preparation of redox-active metal-organic framework ( ra -MOF)-supported Pd nanoparticles (NPs) via the redox couple-driven method is reported, which can yield unprotected metallic NPs at room temperature within 10 min without the use of reducing agents. The Pd@ ra -MOF has been exploited as a precursor of an active catalyst for CO oxidation. Under the CO oxidation reaction condition, Pd@ ra -MOF is transformed into a PdO  x  -NiO  y  /C nanocomposite to generate catalytically active species  in situ , and the resultant nanocatalyst shows sustainable activity through synergistic stabilization.

nanoscale research letters

In situ- generated metal oxide catalyst during CO oxidation reaction transformed from redox-active metal-organic framework-supported palladium nanoparticles