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We have synthesized a variety of monodisperse colloidal GdF 3 :Yb, Er upconversion nanocrystals with different shape, size, and dopants by microwave-assisted synthesis. Typical upconversion emission from Er 3+  was observed. In addition to highly monodisperse spherical particles, we were able to prepare monodispersed rhombic-shaped slices that showed a tendency for self-assembly into stacks.

Monodisperse upconversion GdF3:Yb, Er rhombi by microwave-assisted synthesis