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Structural, magnetic and electronic structural properties ofNi0.2Cd0.3Fe2.5-xAlxO4 ferrites nanoparticles have been studied x-raydiffraction (XRD), transmission electron microscopy (TEM), dc magnetization,and near edge x-ray absorption fine structure spectroscopy (NEXAFS)measurements. Nanoparticles of Ni0.2Cd0.3Fe2.5-xAlxO4 (x = 0.0 - 0.4) ferritewere synthesized using sol-gel method. The XRD and TEM measurements show thatall samples have single phase nature with cubic structure and havenanocrystalline behavior. From the XRD and TEM analysis, it is observed thatparticle size increases with Al doping. DC magnetization measurements inferthat magnetic moment decreases whereas blocking temperature increases withincrease in Al doping. It is observed that the magnetic moment decreases withAl doping which may be due to the dilution of the sublattice by the doping ofAl ions. The NEXAFS measurements performed at room temperature indicates thatFe exist in mixed valence state.

Electronic structure and magnetic properties of Ni0.2Cd0.3Fe2.5-xAlxO4 (x = 0.0 - 0.4) ferrite nanoparticles